Aluminium lithium hydride → HCID 68584177, compound
Reaction equation
[F:1][C:2]1[CH:12]=[CH:11][C:5]([C:6](OCC)=[O:7])=[CH:4][C:3]=1[O:13][C:14]1[CH:19]=[N:18][CH:17]=[CH:16][N:15]=1.[H-].[H-].[H-].[H-].[Li+].[Al+3]>>[F:1][C:2]1[CH:12]=[CH:11][C:5]([CH2:6][OH:7])=[CH:4][C:3]=1[O:13][C:14]1[CH:19]=[N:18][CH:17]=[CH:16][N:15]=1Participants
3
Procedure
The product of Example 128B and LiAlH4 were processed according to the method of Example 124B to provide the product. MS (ESI+) m/z 221(M+H)+.
Workup
- customto provide the product
Sources & evidence
- ORD record
- ord-7d524e6018814e3381b0f96cd465ce35
- Source dataset
- uspto-grants-2013_10
- Patent number
- US08546374B2
Reaction notes
Loading…