Thionyl Chloride → HCID 86082266, compound

HRID 1035034Notes

Reaction equation

HRID 1035034 reaction equation
[F:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8]O)=[CH:4][C:3]=1[O:10][C:11]1[CH:16]=[N:15][CH:14]=[CH:13][N:12]=1.S(Cl)(Cl)=O.[N-:21]=[N+:22]=[N-:23].[Na+]>>[N:21]([CH2:8][C:5]1[CH:6]=[CH:7][C:2]([F:1])=[C:3]([CH:4]=1)[O:10][C:11]1[CH:16]=[N:15][CH:14]=[CH:13][N:12]=1)=[N+:22]=[N-:23]

Participants

4

Reactant 3

HCID 24386Thionyl ChlorideHCID 33557Sodium AzideHCID 68584177HCID 68584177, compound

Product 1

HCID 86082266HCID 86082266, compound

Procedure

The product of Example 128C, thionyl chloride and sodium azide were processed according to the method of Example 115A to provide the product. MS (ESI+) m/z 237 (M+H)+.

Workup

  1. customto provide the product

Sources & evidence

ORD record
ord-f1f5b1cad9fa4b3facbad6add4aa577f
Source dataset
uspto-grants-2013_10
Patent number
US08546374B2

Reaction notes

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