HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 4-(Azidomethyl)-3-fluoropyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | (3-Fluoropyridin-4-yl)methanol | HCID 49760376 | — |
| Product | 4-(Azidomethyl)-3-fluoropyridine | HCID 86082268 | — |
Reaction Steps
The product of Example 129B, thionyl chloride and sodium azide were processed according to the method of Example 115A to provide the product. MS (ESI+) m/z 153 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546374B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-94c961ddd3814f44b0f064a57ad830aa |
| Source note | uspto-grants-2013_10 |