HCID 43087651, compound → HCID 43144871, compound

HRID 1035050Notes

Reaction equation

HRID 1035050 reaction equation
[N:1]1[CH:6]=[CH:5][CH:4]=[C:3]([O:7][C:8]2[N:15]=[CH:14][CH:13]=[CH:12][C:9]=2[C:10]#[N:11])[CH:2]=1>[Ni]>[N:1]1[CH:6]=[CH:5][CH:4]=[C:3]([O:7][C:8]2[C:9]([CH2:10][NH2:11])=[CH:12][CH:13]=[CH:14][N:15]=2)[CH:2]=1

Participants

3

Reactant 1

HCID 43087651HCID 43087651, compound

Product 1

HCID 43144871HCID 43144871, compound

Reagents, catalysts & solvents 1

HCID 935NickelCatalyst

Procedure

The product of Example 139A and Raney/nickel were processed according to the method of Example 131C to provide the product. MS (ESI+) m/z 202 (M+H)+;

Workup

  1. customto provide the product

Sources & evidence

ORD record
ord-8e73fafe33e74a24861f1296d922a9d3
Source dataset
uspto-grants-2013_10
Patent number
US08546374B2

Reaction notes

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