HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrrolidine → HCID 86082298, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | 2-chloro-3-fluoro-4-cyanopyridine | HCID 71757315 | — |
| Product | HCID 86082298 | HCID 86082298 | 94% |
Reaction Steps
Prepared in 94% yield from 2-chloro-4-cyano-3-fluoropyridine and pyrrolidine according to the procedure described for Example 178A. MS (ESI+) m/z 207.9 (M+H) 1H NMR (DMSO-d6) δ 1.91-1.95 (m, 4H), 3.62-3.67 (m, 4H), 7.63 (d, J=4.7 Hz, 1H), 7.98 (d, J=4.7 HZ, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546374B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-28d614263c9f4282813042cf0d3f7afa |
| Source note | uspto-grants-2013_10 |