HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrrolidine → HCID 68583244, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | 2-Chloro-5-fluoropyridine-3-carbonitrile | HCID 23110851 | — |
| Product | HCID 68583244 | HCID 68583244 | 90% |
Reaction Steps
Prepared in 90% yield from the product of Example 169A and pyrrolidine according to the procedure described for Example 178A. MS (ESI+) m/z 192.0 (M+H)+; 1H NMR (DMSO-d6) δ 1.90-1.96 (m, 4H), 3.61-3.65 (m, 4H), 8.05 (dd, J=8.5, 3.0 Hz, 1H), 8.38 (d, J=3.0 Hz, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546374B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-05e0e94009504f9e87c53b6fdeb1e6b2 |
| Source note | uspto-grants-2013_10 |