HRID1035245

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：COc1ccc(-c2nnc(C(=O)N3CC(Oc4ccc(C=O)c(C)c4)C3)o2)cc1

HCID58043156

Benzaldehyde, 4-[[1-[[5-(4-methoxyphenyl)-1,3,4-oxadiazol-2-yl]carbonyl]-3-azetidinyl]oxy]-2-methyl-

C21H19N3O5

HCID66653447

未命名化合物

PRODUCTS

生成物

结构：CCC1(O)CN(Cc2ccc(OC3CN(C(=O)c4nnc(-c5ccc(OC)cc5)o4)C3)cc2C)C1

HCID56597274

未命名化合物

收率 41%

PROCEDURE

实验过程

Using a similar protocol as described in Example 70 employing 73C and 70A as starting materials afforded 100 mg (41%) of 73 as a solid. 1H NMR (500 MHz, CDCl3): δ 0.98 (t, 3H), 1.80 (q, 2H), 2.30 (s, 3H), 2.98 (m, 2H), 3.33 (d, 2H), 3.57 (s, 2H), 3.89 (s, 3H), 4.32 (m, 1H), 4.63 (m, 1H), 4.73 (m, 1H), 5.05 (m, 1H), 5.11 (m, 1H), 6.54 (d, 1H), 6.59 (s, 1H), 7.03 (d, 2H), 7.16 (d, 1H), 8.10 (d, 2H), MS (APCI+) m/z 479 [M+H]+, LC purity: 96%.