HRID1035246

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID139901

4-Hydroxy-3-methylbenzaldehyde

C8H8O2

结构：CS(=O)(=O)OC1CN(C(=O)c2nnc(-c3ccccc3)o2)C1

HCID58043099

未命名化合物

PRODUCTS

生成物

结构：Cc1cc(C=O)ccc1OC1CN(C(=O)c2nnc(-c3ccccc3)o2)C1

HCID58043091

未命名化合物

收率 28%

PROCEDURE

实验过程

Using a similar protocol as described in Example 71A employing 53B and 4-hydroxy-3-methylbenzaldehyde as starting materials afforded 0.8 g (28%) of 74A as a solid. 1H NMR (500 MHz, CDCl3): δ 2.33 (s, 3H), 4.40 (m, 1H), 4.71 (m, 1H), 4.82 (m, 1H), 5.19 (m, 2H), 6.61 (s, 1H), 7.54 (t, 2H), 7.60 (t, 1H), 7.73 (d, 1H), 7.75 (s, 1H), 8.18 (d, 2H), 9.89 (s, 1H).