反应详情

The compound is prepared by the reaction of 3-bromo-7-methoxyquinoline (255 mg, 1.07 mmol, 1.06 eq) and 3-methoxyphenylboric acid (154 mg, 1.01 mmol, 1 eq) according to method A in 4.5 h. Purification by column chromatography with a mixture of hexane/ethyl acetate 9/1 yields the desired product in a yield of 76% (215 mg).

1. customPurification by column chromatography
2. additionwith a mixture of hexane/ethyl acetate 9/1