HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Bromo-6-methoxynaphthalene → 2-Methoxy-6-(4-methoxyphenyl)naphthalene
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Bromo-6-methoxynaphthalene | HCID 78786 | — |
| Edukt | 4-Methoxyphenyl boric acid | HCID 14769994 | — |
| Produkt | 2-Methoxy-6-(4-methoxyphenyl)naphthalene | HCID 11149734 | 56% |
Reaktionsschritte
The compound is prepared by the reaction of 2-bromo-6-methoxynaphthalene (500 mg, 2.11 mmol, 1 eq) with 4-methoxyphenylboric acid (313 mg, 2.12 mmol, 1 eq) according to method A in 5 h. The desired product was precipitated from hexane in a yield of 56% (311 mg).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08546392B2 |
| Quelldatensatz | uspto-grants-2013_10 |
| ORD ID | ord-d5b24212f965472aa7aa059a5de8cdb2 |
| Quellennotiz | uspto-grants-2013_10 |