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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1035610Generated: November 1, 2026

6-Bromo-2-methoxynaphthalene-1-carbaldehyde → HCID 59443478, compound

https://huagongshe.com/reaction/1035610

Reaction equation

Participants

RoleNameHCIDCharge
Reactant6-Bromo-2-methoxynaphthalene-1-carbaldehydeHCID 22018390—
Reactant3-Methoxyphenylboric acidHCID 22173823—
ProductHCID 59443478HCID 5944347886%

Reaction Steps

The compound is prepared by the reaction of 6-bromo-2-methoxy-1-naphthaldehyde (2 g, 7.55 mmol, 1 eq) with 3-methoxyphenylboric acid (1.3 g, 8.30 mmol, 1.1 eq) according to method A. Purification by column chromatography with hexane/ethyl acetate 1/1 as the eluent yielded the desired compound in a yield of 86%, 1.9 g.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08546392B2
Source datasetuspto-grants-2013_10
ORD IDord-b340365be7b94595b1d7e4491be90e08
Source noteuspto-grants-2013_10