HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Bromo-2-methoxynaphthalene-1-carbaldehyde → HCID 59443478, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Bromo-2-methoxynaphthalene-1-carbaldehyde | HCID 22018390 | — |
| Reactant | 3-Methoxyphenylboric acid | HCID 22173823 | — |
| Product | HCID 59443478 | HCID 59443478 | 86% |
Reaction Steps
The compound is prepared by the reaction of 6-bromo-2-methoxy-1-naphthaldehyde (2 g, 7.55 mmol, 1 eq) with 3-methoxyphenylboric acid (1.3 g, 8.30 mmol, 1.1 eq) according to method A. Purification by column chromatography with hexane/ethyl acetate 1/1 as the eluent yielded the desired compound in a yield of 86%, 1.9 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546392B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-b340365be7b94595b1d7e4491be90e08 |
| Source note | uspto-grants-2013_10 |