HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Pyridinylboronic acid → HCID 24970356, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Pyridinylboronic acid | HCID 2734378 | — |
| Reactant | HCID 24950391 | HCID 24950391 | — |
| Product | HCID 24970356 | HCID 24970356 | 59% |
Reaction Steps
The compound is prepared by the reaction of 1-bromo-6-(3-hydroxyphenyl)-naphthalene-2-ol (100 mg, 0.32 mmol, 1 eq) with 3-pyridineboric acid (39 mg, 0.32 mmol, 1 eq) according to method A in 21 h. Purification by column chromatography with hexane/ethyl acetate 7/3 yields the desired compound in a yield of 59%, 59 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546392B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-dc356d4c069746109159ec09eae3714f |
| Source note | uspto-grants-2013_10 |