HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-[3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]acetamide → HCID 25069767, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-[3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]acetamide | HCID 2773989 | — |
| Reactant | HCID 24950391 | HCID 24950391 | — |
| Product | HCID 25069767 | HCID 25069767 | 77% |
Reaction Steps
The compound is prepared by the reaction of 1-bromo-6-(3-hydroxyphenyl)naphthalene-2-ol (150 mg, 0.48 mmol, 1 eq) with N-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)acetamide (124.3 mg, 0.48 mmol, 1 eq) according to method A in 2 h. Purification by column chromatography with hexane/ethyl acetate 8/2 yields the desired compound in a yield of 77%, 136 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546392B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-5c2b1db58753416eb9b6b634ea77059d |
| Source note | uspto-grants-2013_10 |