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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1035620Generated: November 1, 2026

HCID 59443466, compound → HCID 59443443, compound

https://huagongshe.com/reaction/1035620

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 59443466HCID 59443466—
CatalystPalladium hydroxideHCID 9942167—
SolventEthanolHCID 702—
SolventTetrahydrofuranHCID 8028—
ProductHCID 59443443HCID 59443443—

Reaction Steps

A suspension of (E)-3-[3-methoxy-5-(6-methoxynaphthalene-2-yl)phenyl]-N-methylacrylic amide (100 mg, 0.30 mmol, 1 eq) and Pd(OH)2 (2.82 mg) in ethanol (1 ml) and THF (0.4 ml) is stirred for 19 h at RT under a hydrogen atmosphere. Filtration and concentration of the reaction mixture on a rotary evaporator yields the desired product in quantitative yield.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08546392B2
Source datasetuspto-grants-2013_10
ORD IDord-e081813fa9d44cb387fc481be78fbfd2
Source noteuspto-grants-2013_10