Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1035621Generated: October 29, 2026

HCID 59443460, compound → HCID 59443468, compound

https://huagongshe.com/reaction/1035621

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 59443460HCID 59443460—
CatalystPalladium hydroxideHCID 9942167—
SolventEthanolHCID 702—
SolventTetrahydrofuranHCID 8028—
ProductHCID 59443468HCID 59443468—

Reaction Steps

A suspension of (E)-3-[3-methoxy-5-(6-methoxynaphthalene-2-yl)phenyl]-N-phenylacrylic acid amide (70 mg, 0.17 mmol, 1 eq) and Pd(OH)2 (2.5 mg) in ethanol (1 ml) and THF (0.4 ml) is stirred for 20 h at RT under a hydrogen atmosphere. Filtration and concentration of the reaction mixture on a rotary evaporator yields the desired product in quantitative yield (70 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08546392B2
Source datasetuspto-grants-2013_10
ORD IDord-0c39da5de81c4b508a123a175e4931b6
Source noteuspto-grants-2013_10