HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → HCID 59443460, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | HCID 59443486 | HCID 59443486 | — |
| Product | HCID 59443460 | HCID 59443460 | 62% |
Reaction Steps
The compound was prepared by reaction of (E)-3-[3-methoxy-5-(6-methoxy-naphthalene-2-yl)phenyl]acrylic acid (300 mg, 0.89 mmol, 1 eq) with aniline (1 eq) according to method D. Purification by column chromatography with hexane/ethyl acetate 2/1 as the eluent yielded the desired product in a yield of 62%, 227 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546392B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-b237c20dcb264e0c8fc3cd2d73ddc181 |
| Source note | uspto-grants-2013_10 |