Aniline → HCID 59443467, compound

HRID 1035631Notes

Reaction equation

HRID 1035631 reaction equation
[CH3:1][O:2][C:3]1[CH:12]=[CH:11][C:10]2[C:5](=[CH:6][CH:7]=[C:8]([C:13]3[CH:18]=[CH:17][CH:16]=[C:15]([O:19][CH3:20])[CH:14]=3)[CH:9]=2)[C:4]=1/[CH:21]=[CH:22]/[C:23](O)=[O:24].[NH2:26][C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=1>CCOCC>[CH3:1][O:2][C:3]1[CH:12]=[CH:11][C:10]2[C:5](=[CH:6][CH:7]=[C:8]([C:13]3[CH:18]=[CH:17][CH:16]=[C:15]([O:19][CH3:20])[CH:14]=3)[CH:9]=2)[C:4]=1/[CH:21]=[CH:22]/[C:23]([NH:26][C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=1)=[O:24]

Participants

4

Reactant 2

HCID 6115AnilineHCID 59443455HCID 59443455, compound

Product 1

HCID 59443467HCID 59443467, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

The compound was prepared by reaction of (E)-3-(2-methoxy-6-(3-methoxyphenyl)naphthalene-1-yl)acrylic acid (200 mg, 0.60 mmol, 1 eq) with aniline (1 eq) according to method D. Characterization of this compound was not effected. The raw product was directly employed for ether cleavage.

Sources & evidence

ORD record
ord-db0a562bca914fb5a1f7079b39dda257
Source dataset
uspto-grants-2013_10
Patent number
US08546392B2

Reaction notes

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