HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl piperazine-1-carboxylate → HCID 59443464, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl piperazine-1-carboxylate | HCID 143452 | — |
| Reactant | 2-Methoxy-6-(3-methoxyphenyl)-1-naphthoic acid | HCID 59443481 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 59443464 | HCID 59443464 | — |
Reaction Steps
The compound was prepared by reaction of 2-methoxy-6-(3-methoxyphenyl)-1-naphthoic acid (300 mg, 0.97 mmol, 1 eq) with Boc-piperazine (1 eq) according to method D. Characterization of the compound was not effected. The raw product was directly employed for ether cleavage.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546392B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-32d0c7d8366d424782deb7d5ea9c31cb |
| Source note | uspto-grants-2013_10 |