HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron tribromide → 6-(2-Hydroxyphenyl)-2-naphthol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | 2-Methoxy-6-(2-methoxyphenyl)naphthalene | HCID 24829225 | — |
| Product | 6-(2-Hydroxyphenyl)-2-naphthol | HCID 11368353 | 7% |
Reaction Steps
The compound is prepared by reaction of 2-methoxy-6-(2-methoxyphenyl)-naphthalene (150 mg, 0.57 mmol, 1 eq) with boron tribromide (8.5 ml, 8.5 mmol, 15 eq) according to method G. Purification by column chromatography with hexane/ethyl acetate as the eluent yields the desired product in a yield of 7%, 9 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546392B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-56e731c336fe48d4885caad8b708b2ec |
| Source note | uspto-grants-2013_10 |