HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron tribromide → 6-(3-Aminophenyl)-2-naphthalenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | 3-(6-Methoxynaphthalen-2-yl)aniline | HCID 22724074 | — |
| Product | 6-(3-Aminophenyl)-2-naphthalenol | HCID 24827430 | 14% |
Reaction Steps
The compound is prepared by reaction of 3-(6-methoxynaphthalene-2-yl)phenylamine (87.9 mg, 0.35 mmol, 1 eq) with boron tribromide (5 eq) according to method G. Purification by column chromatography with hexane/ethyl acetate 9/1 as the eluent yields the desired product in a yield of 14%, 12 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546392B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-45ec3e1f4f0e4ecca72abe062e6299ca |
| Source note | uspto-grants-2013_10 |