Boron tribromide → HCID 24949875, compound

HRID 1035652Notes

Reaction equation

C[O:2][C:3]1[CH:12]=[CH:11][C:10]2[C:5](=[CH:6][CH:7]=[C:8]([C:13]3[CH:18]=[C:17]([CH3:19])[CH:16]=[C:15]([O:20]C)[CH:14]=3)[CH:9]=2)[CH:4]=1.B(Br)(Br)Br>>[OH:20][C:15]1[CH:14]=[C:13]([C:8]2[CH:9]=[C:10]3[C:5](=[CH:6][CH:7]=2)[CH:4]=[C:3]([OH:2])[CH:12]=[CH:11]3)[CH:18]=[C:17]([CH3:19])[CH:16]=1

Participants

Reactant 2

HCID 25134Boron tribromide

HCID 59443456HCID 59443456, compound

Product 1

HCID 24949875HCID 24949875, compound

Procedure

The compound is prepared by reaction of 2-methoxy-6-(3-methoxy-5-methylphenyl)naphthalene (26 mg, 0.10 mmol, 1 eq) with boron tribromide solution (1 ml, 1 mmol, 10 eq) according to method G. After the processing, the analytically pure compound was obtained (quantitative yield, 25 mg).

Workup

customAfter the processing, the analytically pure compound was obtained (quantitative yield, 25 mg)

Sources & evidence

ORD record: ord-403c808e41ba45fcb656c2dbddafcfd3
Source dataset: uspto-grants-2013_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08546392B2

Reaction notes

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