HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron tribromide → HCID 24950038, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | HCID 59443472 | HCID 59443472 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 24950038 | HCID 24950038 | 92% |
Reaction Steps
The compound is prepared by reaction of 2-(4′,5-dimethoxy-1,1′-biphenyl-3-yl)-6-methoxynaphthalene (40 mg, 0.11 mmol, 1 eq) with boron tribromide solution (1.35 ml, 1.35 mmol, 12 eq) according to method G. After the addition of water, the desired product was obtained as a precipitate in a yield of 92%, 34 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546392B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-4134f92ec45a44c59bc9eeddfbc98010 |
| Source note | uspto-grants-2013_10 |