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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1035654Generated: October 31, 2026

Boron tribromide → HCID 24950039, compound

https://huagongshe.com/reaction/1035654

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBoron tribromideHCID 25134—
ReactantHCID 59443492HCID 59443492—
ProductHCID 24950039HCID 2495003999%

Reaction Steps

The compound is prepared by reaction of 2-methoxy-6-[3-methoxy-5-(6-methoxy-2-naphthyl)phenyl]naphthalene (100 mg, 0.24 mmol, 1 eq) with boron tribromide solution (3.6 ml, 3.6 mmol, 15 eq) according to method G. Purification by column chromatography with hexane/ethyl acetate 9/1 yielded the desired product in a yield of 99%, 90 mg.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08546392B2
Source datasetuspto-grants-2013_10
ORD IDord-6aa1cdad05b249eea4ffa56019afba23
Source noteuspto-grants-2013_10