HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron tribromide → HCID 24950039, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | HCID 59443492 | HCID 59443492 | — |
| Product | HCID 24950039 | HCID 24950039 | 99% |
Reaction Steps
The compound is prepared by reaction of 2-methoxy-6-[3-methoxy-5-(6-methoxy-2-naphthyl)phenyl]naphthalene (100 mg, 0.24 mmol, 1 eq) with boron tribromide solution (3.6 ml, 3.6 mmol, 15 eq) according to method G. Purification by column chromatography with hexane/ethyl acetate 9/1 yielded the desired product in a yield of 99%, 90 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546392B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-6aa1cdad05b249eea4ffa56019afba23 |
| Source note | uspto-grants-2013_10 |