HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron tribromide → 3-Hydroxy-5-(6-hydroxynaphthalene-2-yl)-N-phenylbenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | HCID 59443453 | HCID 59443453 | — |
| Product | 3-Hydroxy-5-(6-hydroxynaphthalene-2-yl)-N-phenylbenzamide | HCID 24950041 | 11% |
Reaction Steps
The compound is prepared by reaction of 3-methoxy-5-(6-methoxynaphthalene-2-yl)-N-phenylbenzamide (300 mg, 0.78 mmol, 1 eq) with boron tribromide solution (5 eq) according to method G. Purification by column chromatography with hexane/dichloromethane 1/99 yielded the desired product in a yield of 11%, 32 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546392B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-1d6300d13bc14f81907aedddce946f36 |
| Source note | uspto-grants-2013_10 |