HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron tribromide → HCID 24950042, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | HCID 59443466 | HCID 59443466 | — |
| Product | HCID 24950042 | HCID 24950042 | 13% |
Reaction Steps
The compound is prepared by reaction of (E)-3-[3-methoxy-5-(6-methoxy-naphthalene-2-yl)phenyl]-N-methylacrylamide (200 mg, 0.58 mmol, 1 eq) with boron tribromide solution (5 eq) according to method G. Purification by preparative thin-layer chromatography with dichloromethane/methanol 90/10 yielded the desired product in a yield of 13%, 25 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546392B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-73d34ec59d3c45469f2d91aada158978 |
| Source note | uspto-grants-2013_10 |