HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron tribromide → HCID 24950043, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | HCID 59443460 | HCID 59443460 | — |
| Product | HCID 24950043 | HCID 24950043 | 14% |
Reaction Steps
The compound is prepared by reaction of (E)-3-[3-methoxy-5-(6-methoxy-naphthalene-2-yl)phenyl]-N-phenylacrylamide (126 mg, 0.31 mmol, 1 eq) with boron tribromide solution (5 eq) according to method G. Purification by preparative thin-layer chromatography with dichloromethane/methanol 98/2 yielded the desired product in a yield of 14%, 17 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546392B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-532fdd6f4169443eb9f9de08ca6dc1f4 |
| Source note | uspto-grants-2013_10 |