Aluminum(III) Chloride → HCID 24950044, compound

Participants

Reaction Steps

The compound is prepared by reaction of 3-[3-methoxy-5-(6-methoxy-naphthalene-2-yl)phenyl]-N-methylpropionamide (47.8 mg, 0.16 mmol, 1 eq) with aluminum trichloride (213.3 mg, 1.60 mmol, 10 eq) according to method F. Purification by preparative thin-layer chromatography with dichloromethane/methanol 98/2 yielded the desired product in a yield of 35%, 16 mg.

Provenance & Evidence