HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron tribromide → HCID 24949874, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | HCID 59443459 | HCID 59443459 | — |
| Product | HCID 24949874 | HCID 24949874 | — |
Reaction Steps
The compound is prepared by reaction of N-[2-methoxy-4-(6-methoxy-2-naphthyl)phenyl]benzamide (49 mg. 0.13 mol, 1 eq) with boron tribromide solution (2.25 ml, 2.25 mmol, 15 eq) according to method G. Purification by preparative thin-layer chromatography with dichloromethane/methanol 95/5 as the eluent yielded the desired product in quantitative yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546392B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-4a4c571b126b4d18a2ec856292240e91 |
| Source note | uspto-grants-2013_10 |