Boron tribromide → HCID 24949872, compound

Participants

Reaction Steps

The compound is prepared by reaction of 3-methoxy-7-(3-methoxyphenyl)-N-phenyl-2-naphthamide (86 mg, 0.22 mol, 1 eq) with boron tribromide solution (4.45 ml, 4.45 mmol, 20 eq) according to method G. Purification by preparative thin-layer chromatography with hexane/ethyl acetate 6/4 as the eluent yielded the desired product in a yield of 50%, 39 mg.

Provenance & Evidence