HRID1035666

反应详情

EQUATION

反应方程式

HRID 1035666 的结构方程式

PROCEDURE

实验过程

The compound is prepared by reaction of 2-methoxy-6-(3-methoxyphenyl)-N-phenyl-1-naphthamide (217 mg, 0.57 mmol, 1 eq) with boron tribromide solution (3.39 mmol, 6 eq) according to method G. Purification by column chromatography with dichloromethane/methanol 95/5 as the eluent yielded the desired product in a yield of 23%, 47 mg.

WORKUP

后处理

  1. customPurification by column chromatography with dichloromethane/methanol 95/5 as the eluent