Boron tribromide → HCID 24950386, compound

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Reaction Steps

The compound is prepared by reaction of 2-methoxy-N,6-bis(3-methoxyphenyl)-1-naphthamide (150 mg, 0.36 mmol, 1 eq) with boron tribromide solution (2.9 ml, 2.9 mmol, 8 eq) according to method G. Purification by column chromatography with dichloromethane/methanol 93/7 as the eluent yielded the desired product in a yield of 75%, 100 mg.

Provenance & Evidence