Boron tribromide → HCID 25070085, compound

Participants

Reaction Steps

The compound is prepared by the reaction of 3-(2-methoxy-6-(3-methoxyphenyl)naphthalene-1-yl)-N-(thiazol-2-yl)benzenesulfonamide (75.3 mg, 0.15 mmol, 1 eq) with boron tribromide solution (14.1 ml, 14.1 mmol, 5 eq) according to method G. Purification by preparative thin-layer chromatography with dichloromethane/methanol 92.5/7.5 as the eluent yielded the desired compound in a yield of 27%, 19 mg.

Provenance & Evidence