Boron tribromide → HCID 25069769, compound

Participants

Reaction Steps

The compound is prepared by the reaction of 3-(2-methoxy-6-(3-methoxyphenyl)naphthalene-1-yl)-N-(5-methyl-1,3,4-thiadiazole-2-yl)benzenesulfonamide (0.28 mmol, 1 eq) with boron tribromide solution (2.8 ml, 2.8 mmol, 10 eq) according to method G. Purification by column chromatography with dichloromethane/methanol 95/5 as the eluent yielded the desired compound in a yield of 47%, 64 mg.

Provenance & Evidence