Dimethylformamide → HCID 59443474, compound

Participants

Reaction Steps

A mixture of 1-bromo-2-methoxy-6-methoxyphenylnaphthalene (850 mg, 2.47 mmol, 1 eq), sodium benzenthiolate (391 mg, 2.96 mmol, 1.2 eq) and anhydrous DMF (10 ml) was refluxed under nitrogen for 11 hours. After cooling to room temperature, the mixture was poured onto ice. The precipitate was filtered off, washed with water and dried. Yield: 385 mg, 42%.

Provenance & Evidence