HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclobutanone → HCID 67126394, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclobutanone | HCID 14496 | — |
| Reactant | Sodium triacetoxyborohydride | HCID 5049666 | — |
| Reactant | HCID 43599637 | HCID 43599637 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67126394 | HCID 67126394 | — |
Reaction Steps
To a solution of EXAMPLE 308A (314 mg) in dichloromethane (5 mL) was added cyclobutanone (70 mg) followed by sodium triacetoxyborohydride (318 mg). The mixture was stirred overnight. The mixture was diluted with dichloromethane (300 mL) and washed with aqueous NaHCO3, water and brine and dried over Na2SO4. After filtration, evaporation of solvent gave the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546399B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-db39083eb77a458e8ba7beb7305739e4 |
| Source note | uspto-grants-2013_10 |