Hydrazine → HCID 178518947, compound

HRID 1036856Notes

Reaction equation

HRID 1036856 reaction equation
[CH:1]1([C:4]2[C:13]3[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=3)[C:7]([N:14]=[C:15]=[S:16])=[CH:6][CH:5]=2)[CH2:3][CH2:2]1.[NH2:17][NH2:18].[C:19](=[O:24])(OC)OC>>[CH:1]1([C:4]2[C:13]3[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=3)[C:7]([N:14]3[C:15]([SH:16])=[N:18][N:17]=[C:19]3[OH:24])=[CH:6][CH:5]=2)[CH2:3][CH2:2]1

Participants

4

Reactant 3

HCID 9321HydrazineHCID 12021Dimethyl CarbonateHCID 565954581-Cyclopropyl-4-isothiocyanatonaphthalene

Product 1

HCID 178518947HCID 178518947, compound

Procedure

1-Cyclopropyl-4-isothiocyanatonaphthalene is reacted with hydrazine and then cyclized in the presence of dimethyl carbonate to form 4-(4-cyclopropylnaphthalen-1-yl)-5-mercapto-4H-1,2,4-triazol-3-ol.

Sources & evidence

ORD record
ord-70f44be58ccf415c9051e99ca12681d8
Source dataset
uspto-grants-2013_10
Patent number
US08546436B2

Reaction notes

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