{1-[4-(6-Fluoro-4-oxo-2-phenyl-4H-chromen-3-yl)-phenyl]-cyclobutyl}-carbamic acid tert-butyl ester → HCID 67067691, compound

Participants

Reaction Steps

Following the procedure used to prepare {1-[4-(6-fluoro-4-oxo-2-phenyl-4H-chromen-3-yl)-phenyl]-cyclobutyl}-carbamic acid tert-butyl ester, 7-iodo-6-phenyl-2,3-dihydro-1,4,5-trioxa-anthracen-8-one (91 mg, 0.225 mmol) was reacted to give the title compound (65 mg, 55%). 1H NMR (400 MHz, CDCl3): δ 7.72 (s, 1H), 7.43-7.14 (m, 9H), 7.00 (s, 1H), 5.03 (s, 1H), 4.43-4.30 (m, 4H), 2.64-2.43 (m, 4H), 2.14-1.98 (m, 1H), 1.91-1.63 (m, 1H), 1.50-1.14 (m, 9H).

Provenance & Evidence