HRID1037312

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID67067816

未命名化合物

结构：COc1c(C=O)ccn2c(=O)n(COCC[Si](C)(C)C)nc12

HCID86671038

未命名化合物

PRODUCTS

生成物

结构：COc1c(C(O)C#Cc2ccccc2)ccn2c(=O)n(COCC[Si](C)(C)C)nc12

HCID67067792

未命名化合物

收率 100%

PROCEDURE

实验过程

Following the procedure used to prepare 1-(2,6-dimethoxy-pyridin-3-yl)-3-phenyl-prop-2-yn-1-ol, 8-methoxy-3-oxo-2-(2-trimethylsilanyl-ethoxymethyl)-2,3-dihydro-[1,2,4]triazolo[4,3-a]pyridine-7-carbaldehyde was reacted to give the title compound (1.05 g, 100%) as a pale yellow gum. LCMS (Method A): RT=4.75 min, [M+H]+=426.

WORKUP

后处理

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