HuagongsheHuagongshe Chemistry Print Report · For research reference only
{1-[4-(6-Fluoro-4-oxo-2-phenyl-4H-chromen-3-yl)-phenyl]-cyclobutyl}-carbamic acid tert-butyl ester → HCID 86671040, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | {1-[4-(6-Fluoro-4-oxo-2-phenyl-4H-chromen-3-yl)-phenyl]-cyclobutyl}-carbamic acid tert-butyl ester | HCID 67067635 | — |
| Reactant | 7-Iodo-8-phenyl-2-(2-trimethylsilanyl-ethoxymethyl)-2H-9-oxa-1,2,3a-triaza-cyclopenta[a]naphthalene-3,6-dione | HCID 86671039 | — |
| Product | HCID 86671040 | HCID 86671040 | 78% |
Reaction Steps
Following the procedure used to prepare {1-[4-(6-fluoro-4-oxo-2-phenyl-4H-chromen-3-yl)-phenyl]-cyclobutyl}-carbamic acid tert-butyl ester, 7-iodo-8-phenyl-2-(2-trimethylsilanyl-ethoxymethyl)-2H-9-oxa-1,2,3a-triaza-cyclopenta[a]naphthalene-3,6-dione was reacted to give the title compound as a pale yellow gum (24 mg, 78%). LCMS (Method A): RT=5.02 min, [M+H]+=655.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546376B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-cd3c14451da54ff3a046015a5d60e869 |
| Source note | uspto-grants-2013_10 |