HuagongsheHuagongshe Chemistry Print Report · For research reference only
{1-[4-(6-Fluoro-4-oxo-2-phenyl-4H-chromen-3-yl)-phenyl]-cyclobutyl}-carbamic acid tert-butyl ester → HCID 67068000, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | {1-[4-(6-Fluoro-4-oxo-2-phenyl-4H-chromen-3-yl)-phenyl]-cyclobutyl}-carbamic acid tert-butyl ester | HCID 67067635 | — |
| Reactant | HCID 67067860 | HCID 67067860 | — |
| Product | HCID 67068000 | HCID 67068000 | 81% |
Reaction Steps
Following the procedure used to prepare {1-[4-(6-fluoro-4-oxo-2-phenyl-4H-chromen-3-yl)-phenyl]-cyclobutyl}-carbamic acid tert-butyl ester, 7-iodo-1-isopropyl-8-phenyl-1H-9-oxa-1,2-diaza-cyclopenta[a]naphthalen-6-one was reacted to give the title compound as a white solid (37.3 mg, 81%). LCMS (Method H): RT=4.70 min, [M+H]+=550.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546376B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-d36f0a0d233444dd87150abef5f32fbc |
| Source note | uspto-grants-2013_10 |