Methanol → HCID 59579722, compound

Participants

Reaction Steps

Into a 250 ml round bottom flask was combined 2-(2-methoxyethyl)-5-nitroisoquinolin-1(2H)-one (1.23 g, 0.00495 mol) palladium/C (0.05 g, 0.0005 mol) and methanol (50 mL, 1 mol). The flask was purged and evacuated with hydrogen twice and the mixture was allowed to stirr under an atmosphere of hydrogen (1 atm) for two hours. The mixture was filtered over Celite and the filtrate reduced in vacuo to yield the title compound as a light brown solid.

Provenance & Evidence