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Cyclopentylacetyl chloride → HCID 178495828、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Cyclopentylacetyl chloride | HCID 3485182 | — |
| 反応物 | 6-Fluoro-3-(2-methoxyethyl)-3H-benzothiazol-2-ylideneamine hydrobromide | HCID 68623548 | — |
| 生成物 | HCID 178495828 | HCID 178495828 | — |
反応手順
The product from Example 113A and cyclopentylacetyl chloride were processed as described for example 11 to afford the title compound. 1H NMR (400 MHz, DMSO-d6) δ ppm 4.54 (d, J=5.76 Hz, 2H) 7.65 (t, J=8.14 Hz, 1H) 7.75 (dd, J=8.81, 2.71 Hz, 1H) 7.83 (dd, J=7.97, 1.53 Hz, 2H) 7.97 (dd, J=8.14, 1.36 Hz, 1H) 8.41 (d, J=3.05 Hz, 1H); MS (ESI+) m/z 337 (M+H)+; Anal. Calculated for C17H21FN2O2S: C, 60.69; H, 6.29; N, 8.33. Found: C, 60.67; H, 6.41; N, 8.25.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08546583B2 |
| 出典データセット | uspto-grants-2013_10 |
| ORD ID | ord-3bd13d3f3881442aa72c4da9b5865513 |
| 出典メモ | uspto-grants-2013_10 |