HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → (Tetrahydro-2H-pyran-4-yl)acetyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | Tetrahydropyran-4-ylacetic acid | HCID 2773575 | — |
| Product | (Tetrahydro-2H-pyran-4-yl)acetyl chloride | HCID 24229747 | — |
Reaction Steps
Commercially available (tetrahydro-pyran-4-yl)-acetic acid and oxalyl chloride were processed as described for example 9A to afford the title compound. MS (DCI/NH3) m/z 159 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546583B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-519e0b281e4242f7bc2346e0218a968f |
| Source note | uspto-grants-2013_10 |