HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-4,5,6,7-tetrahydrobenzothiazole → 5-chloro-2-methoxy-N-(4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-4,5,6,7-tetrahydrobenzothiazole | HCID 18046 | — |
| Reactant | 5-Chloro-o-anisic acid | HCID 76970 | — |
| Product | 5-chloro-2-methoxy-N-(4,5,6,7-tetrahydro-1,3-benzothiazol-2-yl)benzamide | HCID 887954 | — |
Reaction Steps
Commercially available 4,5,6,7-tetrahydrobenzo[d]thiazol-2-amine (Aldrich) and 5-chloro-2-methoxybenzoic acid (Aldrich) were processed using the method described in Example 58 to afford the title compound MS (ESI+) m/z 323 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546583B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-6dbd5fe01a91402eb922745f96586384 |
| Source note | uspto-grants-2013_10 |