HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromoethyl methyl ether → 2-imino-3-(2-methoxyethyl)-6,6-dimethyl-2,3-dihydrofuro[3,4-d]thiazol-4(6H)-one hydrobromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromoethyl methyl ether | HCID 80972 | — |
| Reactant | 2-Amino-6,6-dimethylfuro[3,4-d]thiazol-4(6h)-one | HCID 87518986 | — |
| Product | 2-imino-3-(2-methoxyethyl)-6,6-dimethyl-2,3-dihydrofuro[3,4-d]thiazol-4(6H)-one hydrobromide | HCID 68623117 | — |
Reaction Steps
A mixture of Example 249B and commercially available 2-bromoethyl methyl ether (Aldrich) was processed at 120° C. using the method described in Example 12A to afford the title compound. MS (ESI+) m/z 243 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08546583B2 |
| Source dataset | uspto-grants-2013_10 |
| ORD ID | ord-a5e4a2e3638e4d699a8f6fdb3b1264f9 |
| Source note | uspto-grants-2013_10 |