HRID1037996

反应详情

EQUATION

反应方程式

HRID 1037996 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

2-(5-Nitro-1H-indazol-3-ylmethyl)-isoindole-1,3-dione (0.71 gm) was dissolved in methanol and hydrogenated at 1 atm. using 10% Pd/C (catalytic) for 18 hrs. The catalyst was filtered and the mixture evaporated to obtain 614 mg of title product.

WORKUP

后处理

  1. customfor 18 hrs
  2. filtrationThe catalyst was filtered
  3. customthe mixture evaporated