Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1038068Generated: October 31, 2026

Ammonium formate → HCID 57685732, compound

https://huagongshe.com/reaction/1038068

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAmmonium formateHCID 2723923—
ReactantHCID 57685982HCID 57685982—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 57685732HCID 5768573283.3%

Reaction Steps

A mixture of 3-allyloxy-1-benzyl-pyrrolidine-3-carboxylic acid ethyl ester (145 mg), ammonium formate (126 mg), 10% Pd/C (20 mg) and methanol (4 ml) was refluxed for 40 minutes. The mixture was filtered through Celite, washed with ethyl acetate. The combined filtrate was concentrated and the residue was taken into ethyl acetate, washed with brine and dried over MgSO4. Evaporation of solvent provided the title compound as oil (84 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08546404B2
Source datasetuspto-grants-2013_10
ORD IDord-33e947dba70540de84f996192b4c1314
Source noteuspto-grants-2013_10