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1,4-Dibromo-2,5-difluorobenzene → HCID 57685818、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,4-Dibromo-2,5-difluorobenzene | HCID 67596 | — |
| 反応物 | Tert-butyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1,2,3,6-tetrahydropyridine-1-carboxylate | HCID 4642098 | — |
| 反応物 | HCID 57686416 | HCID 57686416 | — |
| 生成物 | HCID 57685818 | HCID 57685818 | — |
反応手順
The Compound 12AQ was prepared from 4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-3,6-dihydro-2H-pyridine-1-carboxylic acid tert-butyl ester using the procedure as described for the preparation of Compound 4-(2-fluoro-4-pyrimidin-2-yl-phenyl)-3,6-dihydro-2H-pyridine-1-carboxylic acid tert-butyl ester but using 1,4-dibromo-2,5-difluoro-benzene in place of 4-bromo-2-fluoro-1-iodobenzene.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08546404B2 |
| 出典データセット | uspto-grants-2013_10 |
| ORD ID | ord-7d7254c9706745ea8d855bf3186370e5 |
| 出典メモ | uspto-grants-2013_10 |