HCID 57572462, compound → HCID 57572465, compound

HRID 1038285Notes

Reaction equation

HRID 1038285 reaction equation
COC1C(C(N2CCSC2=S)=O)=CC(C(NC)=O)=CC=1C(NC)=O.[CH2:25]([O:32][C:33](=[O:65])[NH:34][CH2:35][CH2:36][CH2:37][NH:38][C:39](=[O:64])[C:40]1[CH:45]=[C:44]([C:46]([N:48]2[CH2:52][CH2:51][S:50][C:49]2=[S:53])=[O:47])[C:43]([O:54][CH3:55])=[C:42]([C:56]([N:58]2CCS[C:59]2=S)=[O:57])[CH:41]=1)[C:26]1[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=1>>[CH2:25]([O:32][C:33](=[O:65])[NH:34][CH2:35][CH2:36][CH2:37][NH:38][C:39](=[O:64])[C:40]1[CH:45]=[C:44]([C:46]([N:48]2[CH2:52][CH2:51][S:50][C:49]2=[S:53])=[O:47])[C:43]([O:54][CH3:55])=[C:42]([C:56](=[O:57])[NH:58][CH3:59])[CH:41]=1)[C:26]1[CH:27]=[CH:28][CH:29]=[CH:30][CH:31]=1

Participants

3

Reactant 2

HCID 57572462HCID 57572462, compoundHCID 57572471HCID 57572471, compound

Product 1

HCID 57572465HCID 57572465, compoundYield 71%

Procedure

Compound 7C was prepared by the same procedure as compound 7A except compound 6C was used instead of compound 6A. Separation and purification were performed as described for compound 7A, pure material was obtained as a thick, bright yellow oil, yield: 71%.

Workup

  1. customSeparation and purification
  2. custompure material was obtained as a thick, bright yellow oil, yield: 71%

Sources & evidence

ORD record
ord-627e7839cbeb488b8030113eed42f2f2
Source dataset
uspto-grants-2013_10
Patent number
US08551453B2

Reaction notes

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