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HRID1038609

反应详情

EQUATION

反应方程式

HRID 1038609 的结构方程式

REACTANTS

反应物

3
结构：CC(C)(C)OC(=O)N1CCNCC1
HCID143452

tert-Butyl piperazine-1-carboxylate

C9H18N2O2

结构：C[C@@H]1CN(C(=O)OC(C)(C)C)[C@@H](C)CN1
HCID11745988

tert-Butyl (2S,5R)-2,5-dimethylpiperazine-1-carboxylate

C11H22N2O2

结构：O=[N+]([O-])c1cc(C(O)(C(F)(F)F)C(F)(F)F)ccc1F
HCID86647210

未命名化合物

PRODUCTS

生成物

1
结构：C[C@@H]1CN(C(=O)OC(C)(C)C)[C@@H](C)CN1c1ccc(C(O)(C(F)(F)F)C(F)(F)F)cc1[N+](=O)[O-]
HCID86647215

未命名化合物

PROCEDURE

实验过程

Similar reaction and treatment as Example 43-b) was conducted except that (2S,5R)-tert-butyl 2,5-dimethylpiperazine-1-carboxylate obtained in Example 14-1-a-2-2) was used in place of 1,1,1,3,3,3-hexafluoro-2-(4-fluoro-3-nitrophenyl)propan-2-ol obtained in Example 43-a) and tert-butyl piperazine-1-carboxylate, and the title compound was obtained as a yellow oil.

WORKUP

后处理

  1. customSimilar reaction and treatment as Example 43-b)